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Results and Conclusions: In this study we have used the

Both proton coupled and proton decoupled (^19)F solid state spectra, recorded using specially designed spectrometer hardware, are presented. The huge gain in resolution afforded by the implementation of proton decoupling allows static and MAS spectra to yield previously inaccessible information pertaining to various NMR parameters of the fluorine nuclei. Advantages of (^1)H(^19)F cross polarisation experiments over single pulse experiments are explained and rotational resonance, dipolar dephasing, T(_1), measurement and spin exchange experiments are presented from which information regarding phenomena such as spin diffusion and polymorphism is gleaned.

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